Analytical Chemistry Experiments

柳军Chongqing University Press · ChinaSep 2023

Rating 3.5
Word count
175 words
Chapters
46
ISBN
9787568933438

Tags

Examinations Lab SafetyData ProcessingEnvironmental MaterialsInstrument UseQuantitative AnalysisPractical ApplicationLab PracticeLab ProjectsOperating StandardsCollege Textbook

Summary

This book consists of three parts: Part 1 introduces the basic knowledge of analytical chemistry experiments; Part 2 introduces the instruments and operations used in analytical chemistry experiments; Part 3 presents the analytical chemistry experiments themselves. The book focuses on experiments in quantitative analysis, with close ties to practical applications in fields such as environment and materials. It can serve as a textbook for undergraduate analytical chemistry laboratory courses in applied chemistry, materials, environmental science and engineering, municipal engineering, geology, and related programs at various higher-education institutions, and may also serve as a reference for related programs at teacher-training colleges.

Editor's review

Published by Chongqing University Press and edited by Liu Jun, Analytical Chemistry Experiments serves as a core laboratory textbook for chemistry and related majors. Its value lies not only in providing standard operating procedures but also in building a progressive learning framework that moves from basic skills to comprehensive design. Rather than simply listing experimental steps, the book integrates error analysis, data processing, and experimental operations, emphasizing the scientific thinking training of "why we do it this way."

Structurally, the book is divided into four modules: basic operation training, quantitative analysis experiments, instrumental analysis experiments, and comprehensive design experiments, covering mainstream methods such as titrimetric analysis, photometric analysis, and electrochemical analysis. Particularly noteworthy is the "Questions and Discussion" section after each experiment, which guides students beyond mechanical operation to a deeper understanding of method principles and influencing factors—a dimension often neglected in traditional laboratory manuals.

As a new textbook published in 2021, the book adds modern instrumental analysis content to traditional analytical methods and introduces application cases such as environmental monitoring and food analysis, reflecting the discipline's trend from the laboratory toward practical application. The textbook's normative requirements for recording and processing experimental data are of significant value in cultivating rigorous research habits in students.

It should be noted that the book is positioned as a professional textbook for higher education and assumes that readers already have a theoretical foundation in analytical chemistry, making it more suitable as a synchronized practical guide for theory courses. For self-learners, it is advisable to first supplement relevant theoretical knowledge before using this book. Overall, this is a rigorously structured laboratory teaching reference that emphasizes the cultivation of thinking, with particular strengths in systematicity and standardization.

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Reading tips

  1. Recommended for use alongside an Analytical Chemistry theory textbook: understand the principles before conducting experiments
  2. Focus on Chapter 1's laboratory safety and data processing standards—often overlooked but critically important
  3. Be sure to complete the discussion questions after each experiment; this is the key step for deepening understanding

About the publisher

Chongqing University Press China · Founded in 1985

Chongqing University Press is a comprehensive university press whose publishing areas span social and cultural studies, industrial technology, finance and economics, medicine, social psychology, and theory. Judging from its catalog, the press publishes both academic works and popular science titles. Representative books include E. H. Gombrich's Shadows: The Depiction of Cast Shadows in Western Art, Magnesium-Based Hydrogen Storage Materials by Pan Fusheng et al., Research on China's Regional Spatial Development Models by Sun Jiuwen, and titles from the Gynecologic Oncology Committee of the Chinese Anti-Cancer Association, such as the Guidelines for Diagnosis and Treatment of Common Gynecologic Malignancies in China (2019) and Bipolar Disorder: What You and Your Family Need to Know. Its authors work in art history, materials science, regional economics, clinical medicine, and social research methods. Public information is limited, but its publishing profile combines academic translation, industrial technology, and practical medical guides.

Contents

  1. 版权信息
  2. 1 分析化学实验基本知识
  3. 1.1 分析化学实验课的目的和要求
  4. 1.2 分析化学实验的一般知识
  5. 1.3 分析化学实验数据的记录、处理和实验报告
  6. 2 分析化学实验仪器及操作
  7. 2.1 分析天平
  8. 2.2 滴定分析的仪器和基本操作
  9. 2.3 重量分析基本操作
  10. 2.4 722S分光光度计
  11. 2.5 756MC型紫外-可见分光光度计
  12. 2.6 MC-960 型荧光分光光度计
  13. 2.7 XJP-821(C)型极谱仪
  14. 2.8 pHS-3C型精密pH计
  15. 2.9 GC-4000A型气相色谱仪
  16. 2.10 ZD-2 型自动电位滴定仪
  17. 3 实验部分
  18. 实验一 分析天平的使用及称量练习
  19. 实验二 工业纯碱总碱度的测定
  20. 实验三 铋、铅含量的连续滴定
  21. 实验四 水泥熟料中SiO2 含量的测定
  22. 实验五 可溶性硫酸盐中硫的测定
  23. 实验六 KMnO4 标准溶液的配制与标定
  24. 实验七 水中溶解氧的测定
  25. 实验八 石灰石中钙、镁含量的测定
  26. 实验九 邻二氮菲分光光度法测定微量铁
  27. 实验十 电位法测定水溶液pH值(设计性实验)
  28. 实验十一 水样中镉的极谱分析
  29. 实验十二 离子选择性电极法测定水中氟含量
  30. 实验十三 乙酸的电位滴定分析及其Ka的测定
  31. 实验十四 水泥熟料中氧化铁、氧化铝的测定(综合性实验)
  32. 实验十五 可溶性氯化物中氯含量的测定(莫尔法)
  33. 实验十六 水样中六价铬的测定
  34. 附录
  35. 附表 1 国际标准相对原子质量
  36. 附录 2 常用化合物的相对分子质量
  37. 附表 3 实验室常用酸、碱溶液的浓度
  38. 附表 4 酸碱指示剂
  39. 附表 5 氧化还原指示剂
  40. 附录 6 金属离子指示剂
  41. 附表 7 实验室中一些试剂的配制方法
  42. 附表 8 常用缓冲溶液的pH值
  43. 附录 9 难溶化合物的溶度积
  44. 附表 10 弱电解质的解离常数
  45. 附表 11 金属离子-氨羧配合剂配合物的稳定常数
  46. 参考文献

FAQ

Does this book require prerequisite coursework? Basic theoretical knowledge of inorganic chemistry and analytical chemistry is required; otherwise, it is difficult to understand the experimental design principles.
Does the book include modern instrumental analysis content? It includes basic instrumental analysis experiments such as UV-visible spectrophotometry and potentiometric analysis, but the depth is limited to the scope of undergraduate teaching.
Is it suitable as a self-study book? The book is designed to accompany university laboratory courses; self-learners need a strong theoretical foundation and should be mindful of laboratory safety constraints.

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About the author

柳军 Author

Liu Jun is an author about whom limited public information is available. Two works can currently be found under this name: Basic Engineering and Analytical Chemistry Experiments, commonly classified under exam preparation. Judging from the titles alone, his writing covers two teaching areas: the fundamentals of civil engineering and analytical chemistry experiments. The former is typically an introductory course for engineering students, while the latter focuses on experimental procedures and data handling in chemistry. Liu Jun's works therefore appear to be textbooks or study aids intended for classroom learning and exam preparation, aimed mainly at students in the relevant fields. Since no details are recorded about his dates of birth and death, nationality, education, or professional positions, his personal background cannot be described. On the available evidence, Liu Jun's contribution lies chiefly in the compilation of these two teaching books, whose practical subject matter follows course requirements and can serve teachers and students in studying and reviewing basic engineering and analytical chemistry experiments.